Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry

Ning Xia; Qin Zhang; De Yao; Guohui Li

doi:10.1007/s00343-008-0475-8

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Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry

OriginalPaper | Updated：2023-05-16

- Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry
- Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry
- 海洋湖沼学报（英文） 2008年26卷第4期页码：475-479
- Affiliations：
  
  1. Qingdao Institute of Marine Geology Chinese Geological Survey
  2. Institute of Geophysical and Geochemical Exploration Chinese Academy of Geological Sciences
  3. Institute of Environmental Science and Technology Shandong University of Technology
- Author bio：
- Funds：
  
  Supported by China Ministry of Science and Technology (2000DEB20081);China Ocean Mineral Resources R&D Association (COMRA) (No. DY105-05-01-05);China Ministry of Education (No.205089) and China National Natural Science Foundation (No.40076015)
- DOI：10.1007/s00343-008-0475-8
  中图分类号：
- 网络首发：2009-01-23，
  
  纸质出版：2008
- Accepted：
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Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry[J]. 海洋湖沼学报（英文）, 2008,26(4):475-479.

Xia, N., Zhang, Q., Yao, D. et al. Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry., Chin. J. Ocean. Limnol. 26, 475–479 (2008). https://doi.org/10.1007/s00343-008-0475-8
Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry[J]. 海洋湖沼学报（英文）, 2008,26(4):475-479. DOI： 10.1007/s00343-008-0475-8.

Xia, N., Zhang, Q., Yao, D. et al. Geochemical analysis of marine sediments using fused glass disc by X-ray fluorescence spectrometry., Chin. J. Ocean. Limnol. 26, 475–479 (2008). https://doi.org/10.1007/s00343-008-0475-8 DOI：

摘要

Abstract

A method was developed for content determination of Na

La and Ce etc. covering 26 major

minor

and trace elements in marine sediment samples using fused glass disc by X-ray Fluorescence spectrometry. Calibration was made using marine sediment certified reference materials and the synthetic standard samples prepared by mixing several marine sediments with stream sediment and carbonate standard samples in different proportions. The matrix effect was corrected using theoretical alpha coefficients

experience coefficients and the scattered radiation as the internal standard (for the trace elements). The accuracy of the method was evaluated by analysis of certified reference materials GBW07314

GBW07334 and GSMS6. The results are in good agreement with the certified values of the standards with RSD less than 2.60%

except for Y

and V with RSD less than 9.0% (n=12).

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references

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